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The result is quite spectacular (Fig. 7. 17). Down to a concentration of 0. 1% of stabiliser, the species M-Na+ govern the spectra. Interestingly, the chances of K+ to unite with M decrease rapidly with decreasing concentration of the latter. 7. 3. 4. 2 Laser-Desorption Ff-lon Cyclotron Resonance {LD/FT-ICR) Mass Spectrometry This sophisticated technique seems to unite the specific advances of other MS techniques discussed to now. FT-ICR can achieve both high resolution and high mass accuracy. Switching from positive to negative ion mass spectral acquisition can be done simply through a software command. At low laser power density, predominantly molecular ions (with addet H+, Na+, K+) are formed while, with higher power density, extensive fragmentation can be obtained for addi- Fig. 7. 13 MALDI-TOF-MS of UVstabilisers (Pasch et al, 10. 2. 5): 1 (above left) Tinuvin 350, Ciba; 2 {above right) 2-(2-hydroxy-3-dodecyl-5-methyl)- phenyltriazole; 3 (below left) 2-(2-hydroxy-3-?-butyl-5-carboxypropionic)phenyltriazole-EO adduct; 4 (below right) mixture of hindered phenols with aliphatic-aromatic phosphite (see Fig. 7. 15) %lnt. M = 323 g/mol [M+H]+ = 324 g/mol Mass/Charge Mass/Charge %lnt. M = 393 g/mol [M+H]+ = 394 g/mol %lnt. %lnt. Mass/Charge Mass/Charge Fig. 7. 17 Left: MALDI-TOF-MS of HDPE, stabilised with Hostanox 03; 1: 0. 4 wt%, 2: 0. 2 wt%, 3: 0. 1 wt%, 4: 0. 01 wt% additive; right: same, stabilised with Hostavin N20; 1:1. 0 wt%, 2: 0. 2 wt%, 3: 0. 1 wt%, 4: 0. 01 wt% additive (Pasch et al. , Lc. ) Mass/Charge M = 795 g/mol [M+Na]+ = 818g/mol [M+K]+ = 834 g/mol M = 364 g/mol [M+Na]+ = 365 g/mol [M+K]+ = 387 g/mol Fig. 7. 16 Structures of the stabilisers in HDPE (see Fig. 7. 17); left: Hostanox O3, right: Hostavin N2o (both Hoechst) (Pasch et al. ,l. c. ) Fig. 7. 15 Structures of the two components of 3 in Fig. 7. 13 (Pasch etal, I. e. ) Fig. 7. 14 Structures of the three peak series in the MALDI-TOF-MS of the EO adduct (3) in Fig. 7. 13 (Pasch et al. ,l. c. ) M = 647 g/mol [M+Na]+ = 670 g/mol [M+K]+ = 686 g/mol M = (660.


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